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5. Tetraalkylammonium trifluoromethanesulfonates [3] Et4N(CF3SO3): Add 5 g of CF3SO3H (33 mmol) to 50 g of 10% Et4NOH (34 mmol), stir it for 30 min, and dry it using a rotating evaporator to get crude Et4N(CF3SO3). Recrystallize it three times from THF and dry in a vacuum. An alternative procedure is to recrystallize the crude product from acetone ethyl ether (1:9) and to dry it for 24 h at 60 8C in a vacuum and in the presence of P2O5, mp 160 161 8C. Bu4N(CF3SO3): Dissolve 9.7 g of Bu4NBr (30 mmol) in 30 ml of water, and, with vigorous stirring, slowly add to it 4.5 g of CF3SO3H (30 mmol). After cooling to room temperature, filter the mixture and wash the precipitate with water. Recover the product remaining in the filtrate by extracting with dichloromethane and add it to the above precipitate. Recrystallize the precipitate twice from dichloromethane ether and dry in a vacuum, mp 111 112.5 8C. As an alternative, the method to neutralize Bu4NOH with CF3SO3H can be employed [18]. 6. Other tetraalkylammonium salts Other tetraalkylammonium salts are also used in electrochemical measurements; they are tetraalkylammonium nitrates, picrates, carboxylates, sulfonates, etc. They can be prepared in the laboratory, by neutralizing the corresponding acid in water with R4NOH just to the equivalence point, removing water, and then drying. If necessary, the products are recrystallized. Some tetraalkylammonium salts form hydrates and are difficult completely to dehydrate. For practical information, see, for example, Ref. [19].

When others might attempt to be diplomatic, to nd words that would assuage an opposing view, if in doing so it caused a compromise to the underlying truth, Merton Miller would have none of it When the spate of so-called derivatives disasters shook up the corporate world several years ago be it Procter & Gamble, Metallgesellschaft, Orange County, or Barings Bank Merton held fast to the underlying reality: These were swaps, he reminded the corporate world You entered into them voluntarily Then, using one of his irrepressible analogies, he would drive the point home I can still hear the echo of his words: A swap is not a robbery, guys! It s not like someone stuck a gun into your ribs and asked for your wallet.

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Milder variants of the HPA axis hyperactivity associated with AN may occur in BN (Coiro et al., 1992; Kennedy et al., 1989). In contrast to AN, relative to healthy comparison women, those with BN exhibit reduced cortisol and sympathetic nervous system (SNS) responses to mental stress (Laessle et al., 1992), suggesting that BN may be associated with stress hyporesponsivity. Reduced levels of central -ED in BN correlate with severity of depressive symptoms (Brewerton et al., 1992), but data regarding peripheral -ED levels are highly inconsistent (Brambilla et al., 1995b; Fullerton et al., 1986; Waller et al., 1986). Opioid antagonists reduce binge purge frequency in both BN and the binge purge subtype of AN, consistent with an auto-addiction model of the disorder (Jonas & Gold, 1986; Marrazzi et al., 1995a). This hypothesis is supported by the nding that in BN the reward value of food is high (Franko et al., 1994; LeGoff et al., 1988) and opioid antagonists reduce both the hedonic value and the amount of food consumed by women with BN, but not simple obesity (Drewnowski et al., 1995). These factors may be important in the aetiology of emotional precipitants to bingeing. Following short-term abstinence from binge purge behaviour, CSF levels of PYY and somatostatin are elevated relative to both acute BN and healthy controls (Kaye et al., 1988, 1990). A relative excess activity in the orexigenic pathways of the hypothalamus might therefore be stimulating over-eating in BN. However, levels of both PYY and NPY in CSF are normal after full recovery, suggesting that this is unlikely to be a trait phenomenon (Gendall et al., 1999).

One of Merton s de ning moments occurred in the aftermath of the 1987 Stock Market Crash during a time that could have meant a death knell to futures As he saw it, it was a battle between New York against Chicago And above all else, Merton was a supreme Chicago patriot and not just for the Chicago Bears It was then that some of the most powerful forces in the nancial establishment were joined by some of the most in uential members of the media and gained the attention of some of the most prominent of cials of government in their attempt to place blame for the crash on Chicago s futures markets Merton Miller s credentials and uncompromising logic stood in their way The most contentious issue of that day was volatility.

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